Iso 8754 reproducibility

TEST STANDARDS ASTM D4294-10,ISO 8754 / 20847, JIS K2541-4 LIMIT OF DITECTION 5 mg/kg (3σ: 3 times the reproducibility standard deviation) when He purge MEASURING RANGE 15 mg/kg to 6 mass% (when He Gas is Used) MEASURING TIME 10 to 990 sec (300 sec is recommended) May 28, 2019 · The test results should be in accordance with ISO 8754 reporting protocol, meaning a tested value at or above 0. : : Figure 7. ISO 10370. 2. TEST STANDARDS ASTM D4294-10,ISO 8754 / 20847, JIS K2541-4 LIMIT OF DITECTION 5 mg/kg (3σ: 3 times the reproducibility standard deviation) when He purge MEASURING RANGE 15 mg/kg to 6 mass% (when He Gas is Used) MEASURING TIME 10 to 990 sec (300 sec is recommended) The reproducibility standard deviation is a core concept defined in the ASTM E 691 - 99 standard. Figure 1. ISO 8754:2003 specifies a method for the determination of the sulfur content of petroleum products, such as naphthas, unleaded motor gasolines, middle distillates, residual fuel oils, base lubricating oils and components. ISO 8754, EN 24260. A gage could be simple, like calipers and ruler. The in vivo testing of the SPF of a sunscreen product according to the procedure in ISO 24444:2010 and AS/NZS 2604:2012 produces a reasonable estimate, but not a highly accurate and precise measure, of the true SPF of the product applied to the skin at a rate of 2 mg Analysis of Sulfur in Petroleum Products According to ASTM D4294 & ISO 8754 using Shimadzu’s EDX-7000 The sulfur content of fuels is widely regulated to reduce atmospheric emissions of sulfur dioxide, or SO2, and other sulfur oxides, or SOx, during combustion of the fuel. Report. 020 0. Iso-inertial tests consisted of lifting as fast as possible four different relative loads (35, 50, 70, 90% 1RM in BP and 45, 60, 75, 90% 1RM in SQ). 4 and regulation 18. 2. The target concentration is represented as S. ISO 4259, Petroleum products — Determination and application of precision data in relation to methods of test. 2019年5月8日 ○IMOはISOに0. de The case depth determination on surfaces hardened components always offers a basis for discussion with regard to the test results found. [**] Fuel oil shall be tested in accordance with ISO 8754:2003. For ISO 8754, repeatability was assessed by performing two sets of 20 analyses (40 total analyses) of the same sample on the same instrument in the same laboratory by the same operator. 3 of this Annex. Table 5 shows the key . These standards are  26 Jul 2019 Refer to ISO 8754:2003 Petroleum products – Determination of sulphur reproducibility of the test method)13, the sulphur content of the fuel. 356. This yields the ideal X-ray source for measuring chlorine and sulfur. According to regulation 11. 1 shows the measurement errors and their causes. over whether a test result meets or exceeds a. In the marine sector, ignition quality is critical for the proper operation of auxiliary systems that operate on distillate fuel (mainly marine gasoil). 1. Butane). Plastics Plastics, polymers, and rubber are combined with diff erent additives to aff ord specifi c properties. The MESA-7220 features a unique, patented design with a close-coupled, doubly curved HOPG X-ray optic. KS M ISO 8754. Determination of sulfur content in crude oil according to ISO 8754 This application note describes the analysis of sulfur contents larger than 0. TS EN ISO 10370 ASTM D 4530 TS EN ISO 2592 ASTM D 92 TS 1233 EN ISO 3016 ASTM D 5950 ASTM D 97 TS 1451 EN ISO 3104 ASTM D 445 TS 1451 EN ISO 3104 ASTM D 445 TS ISO 2909 ASTM D 2270 TS EN ISO 8754 IP 336 Saturated Hydrocarbon Content % wt 50-89 TS 6596 Hydrocarbon Content, Aromatic % wt 15 Max TS 6519 TS 13489 ASTM D 5800 TS 9178 ISO 6618 ASTM D and analysis management tasks defined in ISO 18435 (O&M integration model). Gage Repeatability and Reproducibility is commonly referred to as Gage R&R. Reproducibility Limit is the upper 95% limit calculated for the difference between results repeated with different operators on different instruments. Marine Fuels and Heavy Fuel Oil Test Method/Max Fuel sulphur level Reproducibility A + 0. Repeatability is the variation due to the measurement device. ISO 8754 was prepared by Technical Committee ISO/TC 28, Petroleum products and lubricants . ISO 8754: Sulfur in mineral oil ISO 8754 requires for acceptance the test of the accuracy and reproducibility, running a fresh sample several times on the system. The international standard for marine fuels (ISO 8217) applies the well- established, statistically based, ISO 4259 for the interpretation of test results and it is recommended that IMO should adopt the same approach for the enforcement of the Annex sulphur ISO 8217 stipulates that when there is a dispute. It’s a method that we can use to look at variability in our measurements. preparation of sample will be minimal or inexistent . To quantify repeatability and reproducibility using average and range method, multiple parts, appraisers, and trials are required. out in accordance is ISO 8754:2003 'Petroleum Products – Determination of  1 Sep 2019 Testing fuel oil with ISO 8754 entails the application of repeatability (r) and reproducibility (R). heating, the sulphate is precipitated with barium chloride and determined gravimetrically. should therefore always be recorded. 3, reproducibility is listed as an example or component where the uncertainty of values can be listed. ammonium hydroxide (NH4OH) to precipitate iron ions as ferric oxide (Fe(OH)3). 10 wt% in crude oils, according to international standard ISO 8754, using the Epsilon 4. 3 项Reproducibility 章节,R = 0,0812 (X  content in % m/m as per ISO 8754; and viscosity. The European Standard EN ISO 8754:2003 has the status of a Swedish Standard. Annotations ANNOTATION (informative) [1 December 2014] Here "of measurement" can be deleted without ambiguity: "measurement precision under reproducibility conditions". org) ISO/TR 13843:2017. Sulphur (% m/m). 52% 1. Mass Spec Grade Agilent Ultra Inert Inlet liners provide a robust, reproducible and reliable inert flow path, even when containing CP8754. G Rothwell b H Leander c C Grau d R. 5 Running hours since last regular maintenance Liquid to gas fuel ratio (energy based) as certified at mode point Ratio: % Ratio: [Vol. Whenever national standardization methods of testing MEPC 72: Proposal to mandate ISO sulphur test methods to be discussed further A proposal by China to mandate specific ISO test methods for sulphur, building on a proposal made by IBIA to the IMO earlier this year , has won support to be further considered as the IMO works on measures to ensure uniform implementation of the 0. 1. . Blending "10 The laboratory is to be accredited to ISO/IEC 17025:2017 or an equivalent standard for the performance of the given sulphur content test ISO 8754:2003. The selected gage should be capable of measuring to . 45. Max 4. e. " Tips Although you don't need to purchase the actual catalog to get the ISO number, you may want to purchase one to be sure the material or procedure is exactly the same. -. As a consequence, it seems that this isokinetic device can be used for future sports performance studies and to improve the training process. Vol% ISO code. Regulation No 120 of the Economic Commission for Europe of the United Nations (UN/ECE) — Uniform provisions concerning the approval of internal combustion engines to be installe The focus of my re-creation here is the price contour map shown on the front page of the website for the Electric Reliability Council of Texas, the independent system operator of electric power flow for about 90 percent of Texas residents, as well as the employer of yours truly). An investigation of the repeatability and reproducibility of ISO 11948-1 (the Rothwell method) for measuring the absorption capacity of incontinence pads Author links open overlay panel A. Detta dokument innehåller den officiella engelska versionen av EN ISO 8754:2003. with ISO 3675 or ISO 12185. These two test methods and EN ISO 20847 (Determination of sulfur content of automotive At 15 mg/kg sulfur, this would give a reproducibility of 8. Reproducibility of machine tools’ circularity test according to ISO 230-4 with respect to testing position Article (PDF Available) · January 2017 with 596 Reads How we measure 'reads' ISO 5725:1994 vs MRA:1999 •Dealing with inter-comparisons, ISO 5725 can also be related to the Key Comparisons of the MRA:1999 and to the proficiency tests standards ISO 13528:2005 and ISO 17034:2010. ISO 8754 was prepared by Technical Committee ISO/TC 28, Petroleum products and lubricants. reproducibility, and is considered to be more accurate than the average and range method. 1% 0. Energy-dispersive X-ray fluorescence spectrometry Repeatability and reproducibility are two important requirements in international test methods. 10336. 1 Cetane index – Min 45 40 40 35 ISO 4264 Sulfur b mass % Max 1,00 1,00 1,00 1,50 ISO 8754 or ISO 14596, ASTM D4294; see 6. 59R A – 0. DIN 51 758 Reproducibility of 2. CP7621 DIN H53 N-ISO 9377-2 methods. 2). Guidance for the use of repeatability, reproducibility and trueness estimates in measurement uncertainty evaluation 1 Scope This document gives guidance for — evaluation of measurement uncertainties using data obtained from studies conducted in accordance with ISO 5725-2, and ISO 8754, EN 24260 Flash point Minimum 55 °C ISO 2719 (R = reproducibility). 1. In the case of ISO 8754:2003 R=0. Equation 2: Reproducibility (R), in ppm, according to ASTM D4294 for base oil (a) and diesel fuel (b). 50% sulphur limit. The results of individual  D5453 Repeatability and Reproducibility valuesThe interlaboratory studies to determine the precision of D5453 was divided as follows: Repeatability r” _  TEST STANDARDS. Use of these 8754. Gage R&R 16 / 33 of the repeatability standard deviation and reproducibility standard devi- ation. 2 mg/kg. The reference value of the world wide average sulphur content of residual and distillate fuels supplied for use on board ships should be A wx, where x=r, r ECA, d, d ECA and A wx = A cr as calculated in January of the year following the first three years in which data were collected on the basis of these Guidelines. ISO 14597: Vanadium and Nickel content. • ISO 8754:2003 is the Sulphur test used in ISO 8217, referred to in the Appendix V of MARPOL Annex VI. 2) Setting of the reference values. To design and develop new equipment the industry now uses the most recent International Organization for Standardization ("ISO") standards: ISO 3471-2008; ISO 5700-2013; and ISO 27850-2013. Determination of sulfur content. 12% 0. D4377. *FREE* shipping on qualifying offers. ISO 3733. 53. standard DIN EN ISO 17025, the encreasing of the competitiveness and achieving of high levels of cus- tomer satisfaction. Intermediate Reproducibility (ISO 5725-2:1994 ) is defined as “a measure of reproducibility derived under reproducibility conditions within a single laboratory”. ASTM Table of Contents for reproducibility. The accuracy of the test is Penetračný index -kritérium teplotnej citlivosti asfaltov (Penetration index - criterium of temperature susceptibility of asphalt) Conference Paper (PDF Available) · April 2014 with 62 Reads buy din en iso 8754 e : 2003 petroleum products - determination of sulfur content - energy-dispersive x-ray fluorescence spectrometry from sai global ISO 8754:2003 specifies a method for the determination of the sulfur content of petroleum products, such as naphthas, unleaded motor gasolines, middle distillates, residual fuel oils, base lubricating oils and components. the lowest bleed levels, and the tightest column-to-column reproducibility. NOTE Relevant statistical terms are given in ISO 5725-1:1994 and ISO 5725-2:1994. 02 0. The optical path is under vacuum, so no helium or nitrogen purges are required. same order of magnitude. , to operators’ change, and to their interactions with the measured parts. , Berghauser Straße 62, 42859 Remscheid www. Though the names of the construction equipment covered by the consensus standards have changed over time, OSHA believes that all the equipment listed in current Sec. 10% sulphur should be reported with no more than two decimal places. 1 of MARPOL Annex VI; BS EN ISO 8754:03 Kinematic viscosity at 100 C IP 71 Section 1/97 BS 2000-71:96 sect 1 BS EN ISO 3104:96 Water content IP 74/2000(14) BS 2000-74:00 ISO 3733:99 Manual Sampling Documented In-House Method MP7-9 based on IP 475/05 BS 2000-475:04 BS EN ISO 3170:04 END EN ISO 8501-1:2007Preparation of steel substrates before application of paints and related products - Visual assessment of surface cleanliness - Part 1: Rust grades and preparation grades of uncoated steel substrates and of steel substrates after overall removal of previous coatings (ISO 8501-1:2007). Reproducibility: 0. ISO 8754 [10] describes a standard method by which almost any (energy-dispersive) X-ray fluorescence spectrometer can be calibrated to measure sulphur in petroleum products. Repeatability Limit is the upper 95% limit for the difference between repeated results. M07-053. arnold-horsch. Tables. Attention is drawn to the possibility that some of the elements of this document may be the subject of patent rights. K. ISO 8217 standard that is used for the classification of marine fuels [27] demands the report of the CCI as an indication of the ignition quality. EN ISO 8754 July 2003 ICS 75. ISO 11943 is applied to online particle counters used for contamination analysis of operating systems in the field as well as filter test systems. By re-flecting the results in operation and maintenance plans, the service contributes to stable operation ** Fuel oil shall be tested in accordance with ISO 8754:2003. After filtering and. 05% 0. ASTM D93; ASTM E502; IP 34; ISO 15267; EN ISO 2719; JIS K2265; NF M07- 019;. Per ISO 5725-1 and ISO 5725-6, Repeatability Limit = 2. It is necessary to have an internal precision which is equal or better than the precisions given by the international ISO 8754 and ASTM D4294 standards. To assess the repeatability and reproducibility, use a gage R&R study ( Stat > Quality Tools > Gage Study ). The method is applicable to products having sulfur contents in the range 0,03 % (by mass) to 5,00 % (by mass). 0. iso. J Brooks e Measurements taken during ISO 90 and ISO 120 assessments demonstrated a good degree of reproducibility (see Table 1); when using a sample size of n = 23, reproducibility of peak force associated with T 2 vs T 3 were improved compared to those associated with T 1 vs T 2. IP 470: Aluminium, Silicon, Vanadium, Nickel, Iron, Calcium, zinc and Sodium in residual fuel oil. 00. 8, 2008 (“ISO 3471:2008”), IBR approved for §§ 1926. Sulphur content (% m/m) tested in accordance with ISO 8754. The high voltage, along with multiple ISO 8754: 100 mg/kg – 5 wt%. din en iso 8754 July 1, 2003 Petroleum products - Determination of sulfur content - Energy-dispersive-X-ray fluorescence method (ISO/FDIS 8754:2003), German version prEN ISO 8754:2003 ISO 3471:2008(E), Earth-moving machinery—Roll-over protective structures—Laboratory tests and performance requirements, Fourth Edition, Aug. For ISO 8754  acceptability of a fuel sulphur test result, obtained by using the ISO 8754: 2003 confidence limit which, for a single test result, is given by the reproducibility of. CFPP. 01 – 5wt% The versatility and performance of the Rigaku NEX QC is also demonstrated by its ability to perform other petroleum related applications like multiple elements (P, S, Ca, Zn, and Ba) in able to determine the sulphur in fuels (in accordance with ASTM D4294, EN ISO 20847, ISO 8754 standards) and to analyse the solids, liquids, pastes, suspensions and powders. The Plus model features a Silicon Drift Detector which delivers exceptional short-term repeatability and long-term reproducibility with excellent element peak resolution. 1,50. Additionally, in note 3 under section 5. Standardization (ISO), Institute of Petroleum1 (IP) and Japan LP Gas Association (JLPGA) as reference. b) 0,1 % by mass as from 1 January 2008. 8734 suspension was carried on according to TAPPI Standard Method T230 om-08 and ISO. This robust benchtop analyzer complies with ASTM D4294 and ISO 8754 for For both nickel and vanadium, the ICP repeatability and reproducibility results  [18] and ISO 20884 [19] which both contain comparable reproducibility limits at the 95% probability level for the 20847 and ISO 8754. Flash point. ( www. This second edition cancels and replaces the first edition (ISO 8754:1992), which has been technically revised. Max. 10 Nov 2016 Ash – Reproducibility, Technical, Specification, (Test Method ISO 6245:1982 or equivalent) Results submitted by each of two laboratories  EN ISO 14596 EN ISO 8754 ods, reproducibility or tolerance limits are concerned, it was recommended to use Otherwise the causes are not reproducible in. Metals by AA. (R = reproducibility). – min. They may be the physical supplier or Delivery Company, but not necessarily. CEN. 00 EN ISO 8754 NM380 Flash point °C 60 - ISO 2719 Total sediment wt-% - 0. com. International zero has been taken into account (R = reproducibility). 3 of the ISO/IEC 17025 standard, reproducibility is listed as a value that may be obtained from validated methods. 5. 35. This is because the method does not comply with the tolerance limit guidance according to EN ISO 4259. 69 at 52 CN D4294-IP 336; EN ISO 8754. ISO 5725-3 suggests nomenclature for recording the condi-tions. Evidentiary Considerations for Integration of Biomarkers in Drug Development: A Workshop cosponsored by FDA and - M-CERSI. When applying ISO 4259 to sulphur limits, a fuel could be said to meet the Standard ISO 4259: 1992 ‘Petroleum Products – Determination and application of precision data in relation to methods of tests (incl. +Laboratory accreditation • ISO 17025 - important to ensure the highest of technical standards and test method precision and accuracy are maintained. 0. 080 Supersedes EN ISO 8754:1995 English version Petroleum products - Determination of sulfur content - Energy-dispersive X-ray fluorescence spectrometry (ISO 8754:2003) Produits pétroliers - Détermination de la teneur en soufre - Spectrométrie de fluorescence X dispersive en énergie (ISO 8754:2003) petrol and diesel fuel", the test method EN ISO 8754 is not suitable for determining the sulphur content of petrol or diesel fuels at or below 150ppm and 350ppm, respectively. Sulphur – Reproducibility, (Test Method ISO 8754:1992 or equivalent) Results submitted by each of two laboratories should be considered suspect if they differ by more than 0. 59R". Kinematic viscosity at 80 °C mm²/s 35 49 ISO 3104 Density at 15°C kg/m³ 900 1020 EN ISO 12185 Sulfur wt-% - 1. The Technology. 42% 1. Channel counts. a) Annex 1 as from 1 January 2001; and . Next issue: Part 2 — The practical application of statistics standards for repeatability and reproducibility in interlaboratory studies. ASTM D7751 and ASTM D6481, ISO 8754 Lubricating oil testing Quantify the additives content according to international test methods and norms for Mg, P, S, Cl, Ca, Mo, Zn Base oil Adjust the blending process to elemental concentration of the feed. a. ISO defined repeatability and reproducibility as precision under the repeatability and reproducibility conditions, respectively (see Section 2. 134 1. 7 ISO 10336 ISO 3733 ASTM D 6304 C EUR-Lex Access to European Union law. It then compares measurement variation to the total variability observed, consequently defining the capability of the measurement system. As long as there is no vaccine against our main goal against the COVID-19 pandemic, is to provides a high reliability test to our health partner worldwide. 0​(d). 8) Supplier, Commercial, General, This is the company who issues the Bunker Delivery Receipt for a supply. This document contains the official English version of EN ISO 8754:2003. Water quality — Guidance on validation of microbiological methods ( www. A gage, in this context, is a tool used for measurement. Reproducibility. “Delignification of palm fibre,” BioResources 12(4), 8734-8754. Sixteen male subjects participated in the study in order to verify reproducibility in BP and SQ exercises. The most important requirements test  The current ISO 8217-2012 standard for marine fuels specifies three different distillate grades (DM) and a number of residual grades (RM). 59R (where R is the reproducibility of the test  ISO 3675 or ISO 12185. 40. 2 ISO 8754 ISO 14596 for marine fuel testing listed in ISO 8217:2010, together with reproducibility. Sulphur – Reproducibility, Technical, Specification, (Test Method ISO 8754:1992 or equivalent) Results submitted by each of two laboratories should be considered suspect if they differ by more than 0. (2013). In both cases, the user must decide which reference value 2 will be set. It is a definitive procedure that produces a test result. Minimum 55 °C. instrument repeatability and reproducibility, and instrument calibration and resolution. This standard is described in detail in the following document: "Standard Practice for Conducting an Interlaboratory Study to Determine the Precision of a Test Method", ASTM International, 100 Barr Harbor Drive, PO BOX C700, West Conshohoceken, PA Gage Repeatability and Reproducibility. Declaration . E Test methods for measuring sulphur content, like ASTM D4294 and ISO 8754, have become critical for assessing the value of crude oil. International Organization for Standardization (ISO) has been the accepted standard for marine fuels (bunkers). 053 0. ” “In detecting suspected non-compliance, the sample analysis should be conducted in a uniform and reliable manner as described in the above paragraph. The international standard ISO 5725-2 presents the basic methodology to calculate the repeatability S2 r and the reproducibility S2 R; with those values it is possible to evaluate the homogeneity of the variances through F tests or Chi Square tests. 5% 0. Water (Karl Fischer). Gage reproducibility affects both accuracy and precision. 45% 0. 5%燃料規格策定検討を依頼. Purchase your copy of BS EN ISO 8754:2003, BS 2000-336:2003 as a PDF download or hard copy directly from the official BSI Shop. 49% 0. 055 x (mean Sulphur Content + 0. Therefore, variability between test results needs to be accounted for when determining if the fuel is compliant with the sulphur content standard. 0 acid number 0. 2,00 see 7. A declaration signed and certified by the fuel oil supplier’s representative that the fuel oil supplied is in conformity with the applicable subparagraph of regulation 14. Regulation 14. de – info@arnold-horsch. ISO 4259 as 0. ISO 3733, Petroleum products and bituminous materials — Determination of water — Distillation method. All BSI British Standards available online in electronic and print formats. It could even be a piece of software. 3. However, at a local or national level, the number of available categories can be limited. ISO ( the International Organization for Standardization) is a worldwide federation of ISO 8754 was prepared by Technical Committee ISO/TC 28, Petroleum products   Equation 2: Reproducibility (R), in ppm, according to. Optimise catalyst efficiency by monitoring chlorine levels Jun-2019 C1 (ISO 8178) D2 (ISO 8178) E2 (ISO 8178) E3 (ISO 8178) If no: Is documentation of relevant maintenance provided? 1. 09% EN ISO 14596:2007 1. 59R ISO 8754:2003 1. Prediction of gasoline properties with near infrared spectroscopy. It integrates and analyzes operating information collected during op-eration management and maintenance information collected during maintenance management. 1002(c), specifies performance requirements for metallic roll-over protective structures (ROPS) for earth-moving machinery, as well as a consistent and reproducible means of evaluating the compliance with these requirements by laboratory testing using static loading on a technological reproducibility of the dynamometer. see 7. In order to determine whether marine fuel delivered to and used on board ships is compliant with the sulphur limits specified in the Mandatory Quality Indicators, the fuel verification procedure set out in Appendix VI to Annex VI to the MARPOL Convention shall be used. the relevant sections of ISO 4259 will be used to. 59R (where R is the reproducibility of  “ISO 8754 (1992)” means the method specified by the. August 21, 2015 Lisa M McShane, PhD Biometric Research Branch Division of Cancer Treatment and Diagnosis Home / Method / ISO / 8754 8754. ASTM. Tech Cor 1:1993)’ governs the interpretation of the test results obtained against specification and regulation limits taking into account the precision data. (4) Fuels to power positive-ignition and compression-ignition engines of mobile polluting sources shall comply with requirements specified by . 8 x Repeatability SD. 1001(a) is covered by one of those ISO standards. The recommended method is to use 10 parts, 3 appraisers and 2 trials, for a total of 60 measurements. 13 Test report. The test was repeated one week later. 04 1. M Cottenden a J. Especially differences in crystallinity and crystal structure were focussed. It consists of six parts and the second part, ISO 5725-2 (1994), is the standard for basic method for determination of repeatability and reproducibility of standard measurement method, and is dealing with interlaboratory experiments performed in order to obtain two measures of precision, repeatability and reproducibility. ASTM D4294 for base oil (a ) and diesel fuel (b). 58% 1. 8)%(ww –1) 0 Reproducibility and repeatability v alues for the 12 investigated Reproducibility + ˙ 2 Repeatability and then ˙2 Total = ˙ 2 Parts + ˙ 2 Reproducibility + ˙ 2 Repeatability Note: ˙2 Reproducibility is the variability due to change in experimental conditions, i. ISO 3104 Min 1,400 2,000 3,000 2,000 Density at 15 °C kg/m3 Max – 890,0 890,0 900,0 ISO 3675 or ISO 12185; see 6. 05 for results around 0. 274. 9. 4 In section 5. 15 ISO 10307-1 Carbon residue - Micro method wt-% - 18 ISO 10370 Pour point °C - 30 ASTM D 5950 ISO 3016 Water wt-% - 0. ISO has also developed a new procedure, ISO 11943 [4], for calibration and verification of online particle counting and dilution systems. The standard is listed under number 8217, with recent updates in 2005 and 2010. ISO 13032 - Repeatability The US specification, ASTM D6751, defines biodiesel as mono-alkyl esters of long chain fatty acids derived from vegetable oils and animal fats. -60 to 325/350. Reproducibility increases confidence in the value of our continuous quality assurance processes as well as the trust that users, and anyone interested can put into our released build products (such as ISO and USB images) and our development and release process. Procedures for dealing with biases show how to estimate the standard deviation of the correction so that the sensitivity coefficients are equal to one. The type of alcohol used is not specified. 14, EATA 2013, pp. ISTA Statistics Committee 3 repeatability and reproducibility of a standard measurement method ISO 5725-2 when test result is a numerical value (obtained or computed), where participating laboratories used a Gage Repeatability and Reproducibility (Gage R & R) is a methodology used to define the amount of variation in the measurement data due to the measurement system. technological reproducibility of the dynamometer. 3项Reproducibility 章节,R = 0,0812  operated on the ISO 8178 E-3 test cycle, which is currently used to certify marine ppm [mg/kg] / ISO 8754 or 14596 Reproducibility of the instrument used. 05 to 20. ISO 2719. cessing studies to ensure reproducibility and uniformity of these newer coatings. We focus on R and Python, but [*]Fuel oil shall be tested in accordance with ISO 3675:1998 or ISO 12185:1996. 1926. 9 ‘Intermediate precision’ is also known as ‘within-laboratory reproducibility’. ", [2] as well as effective The Standard is a marketing name for Standard Insurance Company (Portland, Oregon), licensed in all states except New York, and The Standard Life Insurance Company of New York (White Plains, New York), licensed only in New York. 98% 0. Where, as in the usual case, there is a single test result the value of R is that which is stated in the relevant test Precision can have different meanings, depending on what level of variability is included. Measurement repeatability (s repeatability, s r) expresses the closeness of the results obtained with the same sample (or subsamples of the same sample) using the same measurement procedure, same operators, same measuring system, same operating conditions and same location over a short period of time. Reproducibility of hardening depth determination CHD – NHD Arnold Horsch, Arnold Horsch e. % dry] Downstream of heat exchanger Downstream of exhaust gas treatment device In establishment of their limit values the terms of ASTMD 3244 'Defining a basis for petroleum produce quality disputes' have been applied and in fixing a minimum value, a minimum difference of 2R above zero has been taken into account; in fixing a maximum and minimum value, the minimum difference is 4R (R = reproducibility). • ISO 20847 : 30 – 500 mg/kg • ISO 8754 : 100 mg/kg – 5wt% • IP 496: 100 mg/kg – 5wt% • IP 336 : 100 mg/kg – 5wt% • JIS K 2541-4 : 0. [1] In order to ensure accurate and relevant test results, a test method should be "explicit, unambiguous, and experimentally feasible. CP8871. petrol and diesel fuel", the test method EN ISO 8754 is not suitable for determining the sulphur content of petrol or diesel fuels at or below 150ppm and 350ppm, respectively. •Some of the main features of the inter-comparison exercise are different in the three cases. (c) binding sample fall within the reproducibility and/or repeatability of the test method as set out in ISO 4259,  2019年11月18日 ISO 8754:2003硫含量测定标准方法要求采用的仪器种类为能量色散X射线 在这 种情况下应参考该标准第12. Products and availability vary by state and are solely the responsibility of the applicable insurance company. LIMIT OF DITECTION. ASTM D4294-10,ISO 8754 / 20847, JIS K2541-4. Reproducibility was assessed in the same manner as that for ASTM D4294. 1 or 14. Reproducibility and Repeatability Article (PDF Available) in Physiological research / Academia Scientiarum Bohemoslovaca 60(1):203-4; author reply 204-5 · April 2011 with 2,981 Reads Repeatability and reproducibility are the two components of precision in a measurement system. 001”. sulfur cap and the downstream maximum standard of 95 ppm reflected the test reproducibility established by. Petroleum fuels can vary greatly in composition depending on the stock crude and refining process they were subjected to. b. While ISO 8217 takes into account various international requirements for such properties as flash point and sulfur, it is up to the user to identify and ensure compliance with all local, national and regional requirements. ISO 8754. The reproducibility of a single gage is customarily checked by comparing the results of different operators taken at different times. Additive control Verify the additives added into the process for quality control. ‐ EN ISO 16140‐1 and NF EN ISO 16140‐2 (September 2016): Microbiology of the food chain — Method validation Part 1: Vocabulary. 09% Table 1: Uncertainty limits ISO/TS 21748: A new guide to uncertainty estimation using interlaboratory study data S Ellison LGC /Eurachem-UK/2 Overview • Reproducibility and uncertainty estimation • Introduction to ISO TS 21748 /Eurachem-UK/3 What is Measurement Uncertainty? “A parameter, associated with the result of a measurement, • ISO 13032: 8 – 50 mg/kg (NEX QC+ only) The versatility and performance of the Rigaku NEX QC series is also demonstrated by the ability to perform other petroleum For example, ISO 527-5:2009 is "Plastics -- Determination of tensile properties -- Part 5: Test conditions for unidirectional fibre-reinforced plastic composites. I, the fuel oil supplier's representative, hereby certify that the fuel oil supplied is in conformity with regulation 18. 3. This second edition cancels and replaces the first edition (ISO 8754:1992), which has been technically The method, ISO 8754:2003, can be found at the ISO website. This chapter is concerned with the analysis of measurement systems including repeatability, reproducibility, bias, stability, and linearity. Water (% V/V). A test method is a method for a test in science or engineering, such as a physical test, chemical test, or statistical test. Foreword. Available in: en. DIN EN ISO 8754 - 1995-04 Petroleum products - Determination of sulfur content - Energy-dispersive-X-ray fluorescence method (ISO 8754:1992); German version EN ISO 8754:1995. FUEL VERIFICATION PROCEDURE FOR MARPOL ANNEX VI FUEL OIL SAMPLES (Regulation 18. ISO 14596/8754. 308. Or it could be a complex piece of machinery. 55% 0. ISO 4259, Petroleum Products — Determination and Application of Precision Data in Relation to Methods of Test; and ISO 5725, Rubber and Rubber Products — Determination of Precision for Test Method Standards. Excitation: 50 kV X-Ray Tube; 4W Maximum Power; 6 Tube Filter Positions  2020年1月1日 名为:ISO 8754 Petroleum Products - Determination of Sulfur Content A) 对ISO 8754-2003 参考第12. 01  1 Jan 2019 C4 Hydrocarbons (Iso-. 055(X + 0. ISO 8754-2003 (“Petroleum products -- Determination of Sulfur Content need a convenient analyzer capable of accurate and reproducible sulfur readings,  21 Oct 2019 accordance with ISO 8754:2003 by a laboratory that is accredited for exceed the specification limit +0. ISO 14597 Applicable to products having V content in the range of 5 to 1,000 mg/kg, although reproducibility data have only been determined up to 100 mg/kg for V For V content between 5 30 mg/kg: R =5 mg/kg For V content between 31 100 mg/kg: R =10 mg/kg 2. 0% 0. Abstract Preview. 4 on fuel sulphur limits (tested using ISO 8754:2003) reproducibility (R) of the test method multiplied by 0. 1-135) and the definition found in the International Standards Organization (ISO) Standard 1 Apr 2019 For both repeatability and reproducibility as per ISO 8754, the EDX-7000 complied across the entire concentration range of 0. Contipharma-covid19 is the dedicated catalog of CONTIPHARMA (renowed pharmaceutical products distributor since 2016) to help saving lives and overcome the COVID-19 virus. 52% 0. They have broken it down to Residual and Distillate fuels. To analyse crystallinity reproducibility and all the jargon can leave new users feeling overwhelmed, with no idea how to start making their code more reproducible. As a standards development body, the standards products offered include metals, petroleum, construction, environment and many other related standards, test methods, specifications, and guides. 1 and 14. This precision is illustrated graphically in Figure 1 for ultra-low sulfur in gasoline according to ISO 13032 (twenty repeat measurements) and for TIER 3 in Figure 2 (twenty-one repeat measurements over twenty-one days). Sulphur content ISO 8754 0. Logical and correct that this is used. 4 of MARPOL Annex VI, the Administration shall investigate any report of an alleged violation and thereafter promptly inform the Party which made the report, as well as the Organization, of the action taken. It simultaneouslypolarizes,focuses,andmono-chromates the X-ray beam. The MESA-7220 is a compact and lightweight analyzer that can readily measure sulfur and chlorine content in petroleum products down to ppm levels in just 3 minutes. b) Annex 2 as from 1 January 2005. While the reproduction of working drafts or committee drafts in any form for use by participants in the ISO standards solution to determine the acid correction for the heating value, the solution is heated and treated with. Europastandarden EN ISO 8754:2003 gäller som svensk standard. VESTOSINT 3D 8754 HT1 was also printed on an EOSINT P395 at Evonik. The test methods employed to evaluate petrol characteristics were those listed in European standard EN 228:2004 (in particular EN ISO 20884 for sulphur content). A Guide to Reproducible Code covers all the basic tools and information you will need to start making your code more reproducible. 2 ISO 8754. ISO 3735, Crude petroleum and fuel oils — Determination of sediment — Extraction method. ISO 4264. 3 Flash point °C Min 43,0 60,0 60,0 60,0 ISO 2719; see 6. This Handbook follows the ISO guidelines in that biases are corrected (correction may be zero), and the uncertainty component is the standard deviation of the correction. ISO shall not be held responsible for identifying any or all such patent rights. Accuracy (trueness and precision) of measurement methods and results ‘reproducibility’ and ‘repeatability’ are used with varying degrees of consistency in the medical literature. Measurement variation consists of two The IEEE Standard for Floating-Point Arithmetic (IEEE 754) is a technical standard for floating-point arithmetic established in 1985 by the Institute of Electrical and Electronics Engineers (IEEE). The “reliability” of the gage system or similar gage systems to reproduce measurements. Standard: BS EN ISO 8754:2003: Title Identifier: Petroleum products. 1,00. 59, expressed as "the limit plus 0. Total Sediment Existent (% m/m) . The measurement system Annex VI does not specify standard test methods to be used, but the test method of preference for sulphur is currently ISO 8754:2003, 'Petroleum Products - Determination of Sulphur Content - Energy Dispersive X-ray Fluorescence Spectrometry', which is stipulated in marine fuel specification ISO 8217. Test method EN 1601 was employed for the determination of oxygenate content in petrol samples. specification limit, the processes contained in. scope of measuring: from ppm to 100%. 7 ISO 10336 ISO 3733 ASTM D 6304 C Kinematic viscosity at 80 °C mm²/s 48 78 ISO 3104 Density at 15°C kg/m³ 920 1020 EN ISO 12185 Sulfur wt-% - 1. Reproducibility of SPF test results This guideline is currently under review. AccuStandard's Quality System is registered to ISO 9001 and accredited to ISO/ IEC 17025. ISO 8754:2003 Petroleum products - Determination of sulfur content - Energy-dispersive X-ray fluorescence spectrometry. +Representative sample –apply “best practice” ISO 4259 Provides a calculation to describe, with 95% confidence, when a fuel can be considered to meet a specific limit value. Although other types of experiment (such as the split-level exper- iment) are used in certain circumstances for the estimation of precision, they are not dealt with in this part of IS0 5725 but rather are the subject ASTM International provides technical standards to industry worldwide. 8) Supplier, This is the company who issues the Bunker Delivery Receipt for a supply. rights. " In February 2018, IBIA proposed to PPR 5 to define sulphur content in Regulation 2 of Annex VI using the most suitable specific reference test method, ISO 8754 to ensure analysis is done in a uniform and consistent way, including the test result reporting protocol, to avoid differences in application. Sulfur b mass % max. -60 to 305/330. resolve the dispute. °C . fr. 010”. Notwithstanding this measure to ASTM D4294, ISO 20847 and 8754, IP 496 and 336, JIS K 2541-4, as well as ISO 13032. Showing 1–20 of 23 results method. 03 to 4 weight  12. The test results should be in accordance with ISO 8754 reporting protocol, meaning a tested value at or above 0. D4628. 59, expressed as "the limit  International fuel executive for Intertek, retired, and a consultant to ISO TC 28/ SC 4 precision data consisting of the values for repeatability and reproducibility. ISO 5725 (1994) defined precision as the closeness of agreement between independent test results obtained under stipulated conditions. Road Materials and Pavement Design: Vol. 94% 0. Capability of detection -- Part 5: Methodology in the linear and non-linear calibration cases (and Amendment 1:2017). 8. 10. Table 1: On the basis of refer to the ISO 8754:2003. Commonly analyzed as beads, pressed or molded into plaques, typical Compliance with ISO, JIS, and ASTM Plastics Testing Standards As the global demand for plastics increases, it is important to understand the strength properties of plastics, comply with international testing standards, and ensure data reliability. scope: This International Standard specifies a method for the determination of the sulfur content of petroleum products, such as naphthas, unleaded motor gasolines, middle distillates, residual fuel oils, base lubricating oils and components. Gauges should be: i) Accurate (No bias) ii) Precise (Low Variation) Total gage variation includes: Repeatability: Variation in measurements due to a) 0,2 % by mass as from 1 July 2000; and . A2LA maintains additional documents with specific requirements and has checklists for ISO and other standards which are copyright protected. 1001(c) and 1926. 4. Guidance for the use of repeatability, reproducibility and trueness estimates in measurement uncertainty evaluation 1 Scope This document gives guidance for — evaluation of measurement uncertainties using data obtained from studies conducted in accordance with ISO 5725-2, and The EDX2000 Elemental Analyzer (K47910 EDXRF) can analyze a large array of elements from 11Na to 92U in solids, liquids, alloys, powders and thin films. EN 14078: Fatty acid methyl ester (FAME) content. 1 Jan 2020 (where R is the reproducibility of the test method) - the result of test refers as Z in table 2. 093 1. Jul 05, 2013 · In conclusion, the present study showed a high reproducibility of ECC, CON and ISO isokinetic strength for knee extensor and flexor muscles when using REV9000. The standard addressed many problems found in the diverse floating-point implementations that made them difficult to use reliably and portably . analysis of samples will be made by a simple button press . 02% 0. org) ISO/TR 22971:2017. It is the variation that is observed when the same operator measures the same ISO 11843-5:2008. Example: A part has a total tolerance of . Quality Glossary Definition: Gage repeatability and reproducibility (GR&R) Gage repeatability and reproducibility (GR&R) is defined as the process used to evaluate a gauging instrument’s accuracy by ensuring its measurements are repeatable and reproducible. 3 of MARPOL Annex VI and that the sulphur content does not exceed: the limit value given by regulation 14. 3 Reproducibility Reproducibility as defined by ISO 35346 refers to a precision estimate obtained from replicate – The discrimination of the gauge should not exceed 10% of the total part tolerance. 3​(e). EN 14214: Fatty acid methyl esters (FAME) for diesel. ISO 14596. Method D 664 may be used if sufficient sample is available. 50% Delta > Reproducibility R. Beyond the rainbow rotor stage, some 25 sets of pro- duction buckets have now  The standard pays special attention to the lower end of the concentration range covered by ISO 8754, which specifies sulfur contents determination from 0. 59 times the reproducibility value (R); hereafter expressed as 0. For a single test result, this is given by the reproducibility (R) of the test method multiplied by 0. 48% 1. The main reference method adopted for determining the sulphur content shall be in accordance with ISO 8754 or PrEN ISO 14596. 5 mg/kg (3σ: 3 times the reproducibility standard deviation) when  XRF analysis with the LAB-X5000 is repeatable and reproducible for any operator in LAB-X5000 complies with ASTM D4294, ISO 8754, ISO 20847 and IP 33  ASTM D4294, D5059, D6481, ISO 20847, ISO 8754, IP 496, IP 336, JIS K 2541-1 . The layer thickness was always 100 μm and six different sets of parameters (see Table 4) were used to determine the influence on part properties. • ISO 8754 refers to ISO 4259 (determination and  16 Jul 2019 Refer to ISO 8754: 2003 Petroleum products – Determination of Reproducibility (R) calculation in accordance with ISO 4259:2017-2 and as  accordance with ISO 8754:2003 by a laboratory that is accredited for the exceed the specification limit +0. El análisis XRF con el LAB-X5000 es repetible y reproducible para cualquier trabajador. Aug 21, 2015 · Assay validation and reproducibility considerations for biomarkers used in drug development. The multiple stress creep-recovery test: a detailed analysis of repeatability and reproducibility. 12 To be replaced by EN/ISO 6245 with effect of the date of implementation. The definition for "intermodal container," which remains unchanged from the definition in the proposal, reflects a combination of definitions found both in the International Labor Organization (ILO) Code of Practice for Safety and Health in Dock Work (Ex. The results must stay within defined limits: Petrochemical Applications by EDX ISO 8754: Sulfur in mineral oil ISO 8754 requires for acceptance the test of the accuracy and reproducibility, running a sample several times on the system. Cetane index. 3 Reproducibility. 2-11. Agreement and reliability Agreement quantifies how close two measurements made on the same subject are, and is measured on the Aug 23, 2007 · ISO 8754:2003, Petroleum products - Determination of sulfur content - Energy-dispersive X-ray fluorescence spectrometry [ISO/TC 28] on Amazon. 27 ͑X͒0. APPENDIX VI. 59R. So, we have put together this guide to help. ISO5163 ; ISO5165 This ISO document is a working draft or committee draft and is copyright-protected by ISO. Ya sea en el laboratorio, ambientes de producción industrial u  reproducibility, with excellent element peak resolution. These documents are provided from A2LA's electronic document management system to provide the most current document versions. • IP 496: 100 mg/kg – 5 wt%. Part 2: Protocol for the validation of alternative (proprietary) methods against a reference method. " "11 Repeatability (r) calculation in accordance with ISO 4259:2017-2 and as defined in the test method used. We first make clear the distinction between the statistical concepts of agreement and reliability3. 5 The values obtained by Test Methods D 3339 and D 664 may or may not be numerically the same but they should be of the Where X is the mean acid number of sample. Baltimore, MD . VPS has carried out extensive work to determine the whole concentration range precision in terms of repeatability, reproducibility, accuracy and measurement uncertainty. iso 8754 reproducibility

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